synthesis of nanocrystalline batio3 ceramics via hydrothermal condition and structural characterization by hrtem and saed

Authors

s. manafi

department of ceramics, shahrood branch, islamic azad university, shahrood, iran. m. r. rahimipour

materials and energy research center, p.o. box 14155-4777, tehran-iran. i. mobasherpour

materials and energy research center, p.o. box 14155-4777, tehran-iran. a. soltanmoradi

department of ceramics, shahrood branch, islamic azad university, shahrood, iran.

abstract

in the present work, we report a suitable approach for the preparation of batio3 nanostructures via the hydrothermal condition using dolapix et85 as surfactant. the powders were investigated by x-ray diffraction (xrd), scanning election microscopy (sem), energy-dispersive x-ray spectroscopy (edax), field emission transmission electron microscopy (fetem), selected area electron diffraction (saed), high resolution transmission electron microscopy (hrtem) and zetasizer measurement. as a matter of fact, the hydrothermal method guarantees the production of batio3 nanoparticles with desired morphology for commercial applications. in addition, uniform particles, size distribution and purity of samples are highly dependent on the applied hydrothermal condition.

Upgrade to premium to download articles

Sign up to access the full text

Already have an account?login

similar resources

Synthesis of nanocrystalline BaTiO3 ceramics via hydrothermal condition and structural characterization by HRTEM and SAED

In the present work, we report a suitable approach for the preparation of BaTiO3 nanostructures via the hydrothermal condition using Dolapix ET85 as surfactant. The powders were investigated by X-ray diffraction (XRD), scanning election microscopy (SEM), energy-dispersive X-ray spectroscopy (EDAX), field emission transmission electron microscopy (FETEM), selected area electron diffra...

full text

Synthesis of nanocrystalline BaTiO3 ceramics via hydrothermal condition and structural characterization by HRTEM and SAED

In the present work, we report a suitable approach for the preparation of BaTiO3 nanostructures via the hydrothermal condition using Dolapix ET85 as surfactant. The powders were investigated by X-ray diffraction (XRD), scanning election microscopy (SEM), energy-dispersive X-ray spectroscopy (EDAX), field emission transmission electron microscopy (FETEM), selected area electron diffra...

full text

Synthesis and characterization of nanocrystalline CoAPO-5: Structural and morphological analysis by alteration on hydrothermal parameters

Nano-zeolite CoAPO-5 as a member of AFI family, was synthesized via a hydrothermal treatment, and structurally characterized using X-ray diffraction (XRD), scanning electron microscope (SEM), and energy dispersive X-ray analysis (EDAX). The effects of crystallization temperature and time on the structure of these powder products were studied. XRD patterns of the synthesized powders revealed a h...

full text

Synthesis and characterization of nanocrystalline CoAPO-5: Structural and morphological analysis by alteration on hydrothermal parameters

Nano-zeolite CoAPO-5 as a member of AFI family, was synthesized via a hydrothermal treatment, and structurally characterized using X-ray diffraction (XRD), scanning electron microscope (SEM), and energy dispersive X-ray analysis (EDAX). The effects of crystallization temperature and time on the structure of these powder products were studied. XRD patterns of the synthesized powders revealed a h...

full text

synthesis and characterization of nanocrystalline coapo-5: structural and morphological analysis by alteration on hydrothermal parameters

nano-zeolite coapo-5 as a member of afi family, was synthesized via a hydrothermal treatment, and structurally characterized using x-ray diffraction (xrd), scanning electron microscope (sem), and energy dispersive x-ray analysis (edax). the effects of crystallization temperature and time on the structure of these powder products were studied. xrd patterns of the synthesized powders revealed a h...

full text

synthesis and characterization of some macrocyclic schiff bases

ماکروسیکلهای شیف باز از اهمیت زیادی در شیمی آلی و دارویی برخوردار می باشند. این ماکروسیکلها با دارابودن گروه های مناسب در مکانهای مناسب می توانند فلزاتی مثل مس، نیکل و ... را در حفره های خود به دام انداخته، کمپلکسهای پایدار تولید نمایند. در این پایان نامه ابتدا یک دی آلدئید آروماتیک از گلیسیرین تهیه می شود و در مرحله بعدی واکنش با دی آمینهای آروماتیک و یا آلیفاتیک در رقتهای بسیار زیاد منجر به ت...

15 صفحه اول

My Resources

Save resource for easier access later


Journal title:
international journal of nano dimension

جلد ۳، شماره ۲، صفحات ۱۶۳-۱۶۸

Hosted on Doprax cloud platform doprax.com

copyright © 2015-2023